Product
Quality Manufacturer Supply High Purity 99% 2-Bromo-5-nitroaniline 10403-47-1 with Reasonable Price
- Molecular Formula:C6H5BrN2O2
- Molecular Weight:217.022
- Appearance/Colour:Yellow solid
- Vapor Pressure:0.000127mmHg at 25°C
- Melting Point:139-141 °C(lit.)
- Refractive Index:1.669
- Boiling Point:334.5 °C at 760 mmHg
- PKA:0.49±0.10(Predicted)
- Flash Point:156.1 °C
- PSA：71.84000
- Density:1.812 g/cm3
- LogP:3.04390
2-Bromo-5-nitroaniline(Cas 10403-47-1) Usage
InChI:InChI=1/C6H5BrN2O2/c7-5-2-1-4(9(10)11)3-6(5)8/h1-3H,8H2
10403-47-1 Relevant articles
Effect of Hydrogen Bond on Second-Order Nonlinear Optical Property of 2-Alkylcarboxamido-4′-methoxy-4-nitrotolan Derivatives
Kato, Midori,Okunaka, Masaaki,Sugita, Nami,Kiguchi, Masashi,Taniguchi, Yoshio
, p. 583 - 585 (1997)
We have synthesized a series of 2-alkylc...
Factors controlling regioselectivity in the reduction of polynitroaromatics in aqueous solution
Barrows, Susan E.,Cramer, Christopher J.,Truhlar, Donald G.,Elovitz, Michael S.,Weber, Eric J.
, p. 3028 - 3038 (1996)
Regioselectivities in the bisulfide redu...
Cu-mediated selective bromination of aniline derivatives and preliminary mechanism study
Zhao, Hong-Yi,Yang, Xue-Yan,Lei, Hao,Xin, Minhang,Zhang, San-Qi
supporting information, p. 1406 - 1415 (2019/05/01)
A simple and efficient bromination of an...
Iridium-catalyzed intramolecular C–N and C–O/S cross-coupling reactions: Preparation of benzoazole derivatives
Shi, Yajie,Zhou, Qifan,Du, Fangyu,Fu, Yang,Du, Yang,Fang, Ting,Chen, Guoliang
supporting information, (2019/09/10)
The irdium-catalyzed intramolecular aryl...
Polymer-anchored peroxo compounds of molybdenum and tungsten as efficient and versatile catalysts for mild oxidative bromination
Boruah, Jeena Jyoti,Das, Siva Prasad,Borah, Rupam,Gogoi, Sandhya Rani,Islam, Nashreen S.
, p. 246 - 254 (2013/05/23)
A polymer supported peroxomolybdate(VI) ...
Electrophilic bromination of meta-substituted anilines with N-bromosuccinimide: Regioselectivity and solvent effect
Bartoli, Sandra,Cipollone, Amalia,Squarcia, Antonella,Madami, Andrea,Fattori, Daniela
experimental part, p. 1305 - 1308 (2009/12/24)
N-Bromosuccinimide-mediated electrophili...
10403-47-1 Process route
-
-
99-09-2
3-nitro-aniline
-
-
10403-47-1
2-bromo 5-nitroaniline
-
-
53324-38-2
4-bromo-3-nitroaniline
| Conditions | Yield |
|---|---|
|
With
dihydrogen peroxide; potassium bromide;
In
water; acetonitrile;
|
73% 25% |
|
With
tetrabutylammomium bromide; copper(ll) bromide;
In
ethanol;
at 65 ℃;
regioselective reaction;
|
33% 44% |
|
With
sodium hypobromide; water; acetic acid;
man verwandelt in die entsprechenden Acetylderivate, trennt sie durch fraktionierte Krystallisation aus Alkohol und verseift das 6-Brom-3-nitro-acetanilid mit konz.Schwefelsaeure bei 120grad;
|
|
|
With
sodium hypobromide; acetic acid;
|
-
-
N-(2-bromo-5-nitrophenyl)acrylamide
-
-
10403-47-1
2-bromo 5-nitroaniline
| Conditions | Yield |
|---|---|
|
With
potassium acetate; palladium diacetate;
In
dimethyl sulfoxide;
at 100 ℃;
for 10h;
Inert atmosphere;
|
68% |
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