4,4'-[hexane-1,6-diylbis(oxy)]bisbenzonitrile
CAS No.: 94291-61-9
product details:
Purity: 99%
Cost-effective and customizable 4,4'-[hexane-1,6-diylbis(oxy)]bisbenzonitrile 94291-61-9 supplier
- Molecular Formula: C20H20 N2 O2
- Molecular Weight: 320.391
- Boiling Point: 524.3°Cat760mmHg
- Flash Point: 200.1°C
- PSA： 66.04000
- Density: 1.14g/cm3
- LogP: 4.44816
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94291-61-9 Process route
-
-
629-03-8
1 ,6-dibromohexane
-
-
767-00-0
4-cyanophenol
-
-
94291-61-9
4,4'-(hexane-1,6-diylbis(oxy))dibenzonitrile
| Conditions | Yield |
|---|---|
|
4-cyanophenol;
With
sodium;
In
ethanol;
for 1h;
Reflux;
1 ,6-dibromohexane;
In
ethanol;
for 3h;
Reagent/catalyst;
Solvent;
|
94.52%
|
|
With
potassium carbonate;
In
acetonitrile;
Reflux;
|
86.2%
|
|
4-cyanophenol;
With
sodium hydroxide;
In
ethanol; water;
at 20 - 80 ℃;
for 2h;
Industrial scale;
1 ,6-dibromohexane;
In
ethanol; water;
at 80 - 85 ℃;
Concentration;
Industrial scale;
|
81%
|
|
With
sodium ethanolate;
for 48h;
Heating;
|
|
|
With
potassium carbonate;
In
N,N-dimethyl-formamide;
Reflux;
|
|
|
With
caesium carbonate;
In
acetone;
for 14h;
Reflux;
Inert atmosphere;
|
-
-
629-11-8
1,6-hexanediol
-
-
4-cyano-N,N,N-trimethylanilinium trifluoromethansulfonate
-
-
94291-61-9
4,4'-(hexane-1,6-diylbis(oxy))dibenzonitrile
| Conditions | Yield |
|---|---|
|
1,6-hexanediol;
With
potassium tert-butylate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 25 ℃;
for 0.166667h;
Inert atmosphere;
Schlenk technique;
4-cyano-N,N,N-trimethylanilinium trifluoromethansulfonate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 25 ℃;
for 3h;
Inert atmosphere;
Schlenk technique;
|
70%
|
94291-61-9 Upstream products
-
629-03-8
1 ,6-dibromohexane
-
3328-57-2
sodium 4-cyanophenolate
-
767-00-0
4-cyanophenol
-
629-11-8
1,6-hexanediol
94291-61-9 Downstream products
-
50357-46-5
4,4'-hexanediyldioxy-bis-benzamidine; dihydrochloride
-
1448-62-0
4,4'-iminoethyl-1,6-diphenoxyhexane
-
1246-08-8
1.6-Bis- <4-thiocarbamoyl-phenoxy> -hexan
-
125880-54-8
C20 H18 N4 O6
